Hanna-instruments HI 83206 Manual de usuario

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Instruction Manual
HI 83206
Multiparameter Bench
Photometer
for Environmental Testing
www.hannainst.com
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Pagina 1 - HI 83206

1Instruction ManualHI 83206Multiparameter BenchPhotometerfor Environmental Testingwww.hannainst.com

Pagina 2 - TABLE OF CONTENTS

10• Pay attention to push the cuvette completely down in the holder and to align the white point on thecap to the indexing mark on the meter.• In orde

Pagina 3 - GENERAL DESCRIPTION

11METHOD REFERENCE TABLEMethod Method Pagedescription1 Ammonia MR 172 Ammonia LR 193 Free Chlorine 214 Total Chlorine 245 Chromium VI HR 276 Chromium

Pagina 4 - SPECIFICATIONS

12POWER CONNECTION AND BATTERY MANAGEMENTThe meter can be powered from an AC/DC adapter (included) or from the built-in rechargeable battery.Note: Alw

Pagina 5

13DATA MANAGEMENTThe instrument features a data log function to help you keep track of all your analysis. The data log canhold 200 individual measurem

Pagina 6 - FUNCTIONAL DESCRIPTION

14In the Setup mode the instrument’s parameters can be changed. Some parameters affect the measuringsequence and others are general parameters that ch

Pagina 7 - KEYPAD DESCRIPTION

15Date / TimeThis option is used to set the instrument’s date and time.Press the Modify key to change the date/time.Press the W X functional keys to h

Pagina 8

16HI 83206 offers an interactive contextual help mode that assists the user at any time.To access the help screens press HELP.The instrument will disp

Pagina 9 - USING CUVETTES

17Ammonia MRSPECIFICATIONSRange 0.00 to 10.00 mg/LResolution 0.01 mg/LAccuracy ±0.05 mg/L ±5% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLight

Pagina 10 - INTERFERENCES

18• Remove the cuvette.• Add 4 drops of HI 93715A-0 First reagent (6 drops forseawater analysis). Replace the cap and mix the solution.• Add 4 drops o

Pagina 11 - HEALTH & SAFETY

19Ammonia LRSPECIFICATIONSRange 0.00 to 3.00 mg/LResolution 0.01 mg/LAccuracy ±0.04 mg/L ±4% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLight S

Pagina 12 - OPERATIONAL GUIDE

2Dear Customer,Thank you for choosing a Hanna product. Please read this instruction manual carefully before using theinstrument. This manual will prov

Pagina 13 - CHEMICAL FORM

20Ammonia LR• Remove the cuvette.• Add 4 drops of HI 93700A-0 First reagent (6 drops forseawater analysis). Replace the cap and mix the solution.• Add

Pagina 14 - SETUPSETUP

21FREE CHLORINEFREE CHLORINEFREE CHLORINEFREE CHLORINEFREE CHLORINESPECIFICATIONSRange 0.00 to 2.50 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3% of

Pagina 15

22Free Chlorine• Press the Zero key. The meter will show “-0.0-” when the meter is zeroed and ready for measurement.• Remove the cuvette.Powder reagen

Pagina 16 - HELP MODEHELP MODE

23• Reinsert the cuvette into the instrument.• Press Read to start the reading. The instrument displays the results in mg/L of free chlorine.INTERFER

Pagina 17 - AMMONIA MEDIUM RANGE

24Total ChlorineTOTAL CHLORINESPECIFICATIONSRange 0.00 to 3.50 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3% of reading at 25 °CTypical EMC ±

Pagina 18

25Total Chlorine• Press the Zero key. The meter will show “-0.0-” when the meter is zeroed and ready for measurement.• Remove the cuvette.Powder reage

Pagina 19 - AMMONIA LOW RANGE

26• Press Timer and the display will show the countdown prior to the measurement or, alternatively, waitfor 2 minutes and 30 seconds and press Read. W

Pagina 20

27Chromium VI HRCHROMIUM VI HIGH RANGESPECIFICATIONSRange 0 to 1000 μg/LResolution 1 μg/LAccuracy ±5 μg/L ±4% of reading at 25 °CTypical EMC ±1 μg/LDe

Pagina 21 - FREE CHLORINE

28• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternatively, waitfor

Pagina 22 - Free Chlorine

29Chromium VI LRCHROMIUM VI LOW RANGESPECIFICATIONSRange 0 to 300 μg/LResolution 1 μg/LAccuracy ±1 μg/L ±4% of reading at 25 °CTypical EMC ±1 μg/LDevi

Pagina 23

3PRELIMINARY EXAMINATIONPlease examine this product carefully. Make sure that the instrument is not damaged. If any damageoccurred during shipment, pl

Pagina 24 - TOTAL CHLORINE

30• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternatively, waitfor

Pagina 25 - Total Chlorine

31Color of WaterCOLOR OF WATERSPECIFICATIONSRange 0 to 500 PCU (Platinum Cobalt Units)Resolution 1 PCUAccuracy ±10 PCU ±5% of reading at 25 °CTypical

Pagina 26

32Color of Water• Fill the second cuvette up to the mark with unfiltered sampleand replace the cap. This is the apparent color.• Filter 10 mL of sampl

Pagina 27 - CHROMIUM VI HIGH RANGE

33Copper HRCOPPER HIGH RANGESPECIFICATIONSRange 0.00 to 5.00 mg/LResolution 0.01 mg/LAccuracy ±0.02 mg/L ±4% of reading at 25 °CTypical EMC ±0.01 mg/L

Pagina 28

34Copper HR• Remove the cuvette.• Add the content of one packet of HI 93702-0 Bicinchoninate.Replace the cap and shake gently for about 15 seconds.• R

Pagina 29 - CHROMIUM VI LOW RANGE

35Copper LRCOPPER LOW RANGESPECIFICATIONSRange 0 to 1000 μg/LResolution 1 μg/LAccuracy ±10 μg/L ±5% of reading at 25 °CTypical EMC ±1 μg/LDeviationLig

Pagina 30

36Copper LR• Remove the cuvette.• Add the content of one packet of HI 95747-0 Bicinchoninate.Replace the cap and shake gently for about 15 seconds.• R

Pagina 31 - COLOR OF WATER

37Cyanuric AcidCYANURIC ACIDSPECIFICATIONSRange 0 to 80 mg/LResolution 1 mg/LAccuracy ±1 mg/L ±15% of reading at 25 °CTypical EMC ±1 mg/LDeviationLigh

Pagina 32 - Color of Water

38Cyanuric Acid• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternati

Pagina 33 - COPPER HIGH RANGE

39MolybdenumMOLYBDENUMSPECIFICATIONSRange 0.0 to 40.0 mg/LResolution 0.1 mg/LAccuracy ±0.3 mg/L ±5% of reading at 25 °CTypical EMC ±0.1 mg/LDeviationL

Pagina 34

4PRINCIPLE OF OPERATIONAbsorption of light is a typical phenomenon of interaction between electromagnetic radiation and matter.When a light beam cross

Pagina 35 - COPPER LOW RANGE

40• Fill one graduated mixing cylinder up to the 25 mLmark with the sample.• Add the content of one packet of HI 93730A-0molybdenum reagent, close the

Pagina 36

41Molybdenum• Press Timer and the display will show the countdown prior to the measurement or, alternatively, waitfor 5 minutes and press Read. When t

Pagina 37 - CYANURIC ACID

42Nickel HRSPECIFICATIONSRange 0.00 to 7.00 g/LResolution 0.01 g/LAccuracy ±0.07 g/L ±4% of reading at 25 °CTypical EMC ±0.02 g/LDeviationLight Source

Pagina 38 - Cyanuric Acid

43Nickel HR• Remove the cuvette and add the content of one packet ofHI 93726-0 reagent. Replace the cap and shake gentlyuntil completely dissolved.• R

Pagina 39 - MOLYBDENUM

44Nickel LRNICKEL LOW RANGESPECIFICATIONSRange 0.000 to 1.000 mg/LResolution 0.001 mg/LAccuracy ±0.010 mg/L ±7% of reading at 25 °CTypical EMC ±0.001

Pagina 40 - Molybdenum

45Nickel LR• Press Timer and the display will show a countdown prior to adding reagent C or, alternatively, waitfor 15 minutes. Add one packet of HI 9

Pagina 41

46INTERFERENCESInterference may be caused by:Co2+ must not be presentFe2+ must not be presentAl3+ above 32 mg/LCa2+ above 1000 mg/L (as CaCO3)Cd2+ abo

Pagina 42 - NICKEL HIGH RANGE

47NitrateSPECIFICATIONSRange 0.0 to 30.0 mg/LResolution 0.1 mg/LAccuracy ±0.5 mg/L ±10% of reading at 25 °CTypical EMC ±0.1 mg/LDeviationLight Source

Pagina 43

48Nitrate• Replace the cap and immediately shake vigorously upand down for exactly 10 seconds. Continue to mix byinverting the cuvette gently for 50 s

Pagina 44 - NICKEL LOW RANGE

49Nitrite HRNITRITE HIGH RANGESPECIFICATIONSRange 0 to 150 mg/LResolution 1 mg/LAccuracy ±4 mg/L ±4% of reading at 25 °CTypical EMC ±1 mg/LDeviationLi

Pagina 45 - Nickel LR

5Where:-log I/Io= Absorbance (A)Io= intensity of incident light beamI = intensity of light beam after absorptionελ= molar extinction coefficient at wa

Pagina 46

50Nitrite HR• Add the content of one packet of HI 93708-0 reagent.Replace the cap and shake gently until completely dissolved.• Reinsert the cuvette i

Pagina 47 - MEASUREMENT PROCEDURE

51SPECIFICATIONSRange 0.00 to 1.15 mg/LResolution 0.01 mg/LAccuracy ±0.06 mg/L ±4% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLight Source Tung

Pagina 48

52• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternatively, waitfor

Pagina 49 - NITRITE HIGH RANGE

53Dissolved OxygenSPECIFICATIONSRange 0.0 to 10.0 mg/LResolution 0.1 mg/LAccuracy ±0.4 mg/L ±3% of reading at 25 °CTypical EMC ± 0.1 mg/LDeviationLigh

Pagina 50 - Nitrite HR

54Dissolved Oxygen• Let the sample stand and the flocculent agent will start to settle.• After approximately 2 minutes, when the upper half of the bot

Pagina 51 - NITRITE LOW RANGE

55pHpHSPECIFICATIONSRange 6.5 to 8.5 pHResolution 0.1 pHAccuracy ±0.1 pH at 25 °CTypical EMC ±0.1 pHDeviationLight Source Tungsten lamp with narrow ba

Pagina 52

56pH• Remove the cuvette and add 5 drops of HI 93710-0 PhenolRed Indicator. Replace the cap and mix the solution.• Reinsert the cuvette into the instr

Pagina 53 - DISSOLVED OXYGEN

57Phosphate HRPHOSPHATE HIGH RANGESPECIFICATIONSRange 0.0 to 30.0 mg/LResolution 0.1 mg/LAccuracy ±1 mg/L ±4% of reading at 25 °CTypical EMC Dev. ±0.1

Pagina 54

58Phosphate HR• Add the content of one packet of HI 93717B-0 PhosphateHR Reagent B to the cuvette. Replace the cap and shakegently until completely di

Pagina 55

59Phosphate LRPHOSPHATE LOW RANGESPECIFICATIONSRange 0.00 to 2.50 mg/LResolution 0.01 mg/LAccuracy ±0.04 mg/L ±4% of reading at 25 °CTypical EMC Dev.

Pagina 56

6INSTRUMENT DESCRIPTION1) Open Cuvette Lid2) Indexing mark3) Cuvette point4) Liquid Crystal Display (LCD)5) Splash proof keypad6) ON/OFF power switch7

Pagina 57 - PHOSPHATE HIGH RANGE

60Phosphate LR• Reinsert the cuvette into the instrument.• Press Timer and the display will show the countdown prior to the measurement or, alternativ

Pagina 58

61PhosphorusPHOSPHORUSSPECIFICATIONSRange 0.0 to 15.0 mg/LResolution 0.1 mg/LAccuracy ±0.3 mg/L ±4% of reading at 25 °CTypical EMC Dev. ±0.2 mg/LLight

Pagina 59 - PHOSPHATE LOW RANGE

62Phosphorus• Add the content of one packet of HI 93706B-0 PhosphorusReagent B (Amino Acid) to the cuvette. Replace the capand shake gently until comp

Pagina 60 - Phosphate LR

63SilicaSILICASPECIFICATIONSRange 0.00 to 2.00 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLight

Pagina 61 - PHOSPHORUS

64Silica• Place the cuvette into the holder and close the lid.• Press the Zero key. The display will show “-0.0-” when the meter is zeroed and ready f

Pagina 62

65• Press the Chem Frm key to convert the result in mg/L of Silicon (Si).• Press  or  to return to the measurement screen.INTERFERENCESInterference

Pagina 63

66SilverSILVERSPECIFICATIONSRange 0.000 to 1.000 mg/LResolution 0.005 mg/LAccuracy ±0.020 mg/L ±5% of reading at 25 °CTypical EMC ± 0.001 mg/LDeviatio

Pagina 64

67Silver• Add exactly 1.0 mL of HI 93737B-0 Buffer reagent to the secondbeaker (the sample) and swirl gently to mix. Press Timer and thedisplay will s

Pagina 65

68Silver• Press the Zero key. The display will show “-0.0-” when the meter is zeroed and ready formeasurement.• Fill a second cuvette up to the mark w

Pagina 66

69ZincZINCSPECIFICATIONSRange 0.00 to 3.00 mg/LResolution 0.01 mg/LAccuracy ±0.03 mg/L ±3% of reading at 25 °CTypical EMC ±0.01 mg/LDeviationLight Sou

Pagina 67

7KEYPAD DESCRIPTIONThe keypad contains 8 direct keys and 3 functional keys with the following functions:Press to perform the function displayed above

Pagina 68

70INTERFERENCESInterference may be caused by:Aluminum above 6 mg/LCadmium above 0.5 mg/LCopper above 5 mg/LIron above 7 mg/LManganese above 5 mg/LNick

Pagina 69 - REQUIRED REAGENT

71The instrument shows clear warning messages when erroneous conditions appear and when measured values areoutside the expected range. These messages

Pagina 70

72Description Range MethodAmmonia MR 0.00 to 10.00 mg/L NesslerAmmonia LR 0.00 to 3.00 mg/ L NesslerChlorine, Free 0.00 to 2.50 mg/ L DPDChlorine, Tot

Pagina 71 - ERRORS AND WARNINGS

73Nitrate 0.0 to 30.0 mg/L Cadmium ReductionNitrite HR 0 to 150 mg/L Ferrous SulfateNitrite LR 0.00 to 1.15 mg/L DiazotizationOxygen, Dissolved 0.0 to

Pagina 72 - STANDARD METHODS

74HI 93722-01 100 cyanuric acid testsHI 93722-03 300 cyanuric acid testsHI 93723-01 100 chromium VI HR testsHI 93723-03 300 chromium VI HR testsHI 937

Pagina 73 - ACCESSORIES

75WARRANTYAll Hanna Instruments meters are warranted for two years against defects in workmanship and materialswhen used for its intended purpose and

Pagina 74

76Printed in EUROPE(ROMANIA)Hanna Instruments Inc.Highland Industrial Park584 Park East DriveWoonsocket, RI 02895 USATechnical Support for CustomersTe

Pagina 75 - HANNA LITERATURE

8The instructions listed below should be carefully followed during testing to ensure most accurate results.• Color or suspended matter in large amount

Pagina 76 - MAN83206 04/10

9• Proper use of the powder reagent packet:(a) use scissors to open the powder packet;(b) push the edges of the packet to form a spout;(c) pour out th

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