Hanna-instruments HI 9017 Manual de usuario

HI9017 - HI9218HI9219 - HI9318MicroprocessorBench-toppH Meters withRS232CInstruction ManualPAPERPRINTCLEARONOFFDATERANGECALABC789456423+/-.PGMCON+/-TE

10SPECIFICATIONS HI9318Ranges pH 0.00 to 14.00ISE 0 to ±399.9 mVORP 0 to ±1999 mV °C -10.0 to 125.0Resolution pH 0.01ISE 0.1mVORP 1 mV°C 0.1Accuracy

111) BNC male connector for single or combination electrode. Willaccept any pH or ORP electrode with a standard BNC connector.2) Jack bush connector

12+-Power connectionPlug the 12VDC adapter (HI710005 or HI710006) into the DC socket(#7).Plug the adapter into the mains.Note: The instrument uses the

13pH°C4 cm(1½")TAKING PH MEASUREMENTSMake sure that the instrument has been calibrated for pH beforetaking pH measurements (see page 18).Connect

1432.7TEMP°CFor the rinsing process, it is recommended to use a liberal amount ofthe next solution to be measured.Using refillable electrodesUnscrew t

157 +/-3.TEMPºCDOWNºCUP°C°CWith negative temperature values (e.g. -7.3°C) use the +/- key• press 7• press decimal point• press 3• press +/-• press TEM

16TAKING TEMPERATURE MEASUREMENTSTaking a temperature measurement is very easy.Turn the instrument ON.Make sure the temperature probe is connected and

17FOR HI 9318 ONLYPress PRINT key to get a printout at any time.All the printouts will be complete with date, time, sample No., tem-perature and mV va

18IMPORTANTThe instrument's pH range should be re-calibrated:••••• When the meter is new.••••• Whenever the pH electrode is replaced.••••• At lea

19• Immerse the pH electrode and the ATC probeinto pH7.01 buffer solution. Shake briefly andwait 1-2 minutes for thermal equilibrium.Note: the electro

2Dear Customer,Thank you for choosing a Hanna Instruments Product.Please read this instruction manual carefully before using the instru-ment.This manu

20• Rinse the electrode and the temperature probebefore immersing them into pH 4.01 or pH10.01calibration buffer, shake briefly and wait forthermal eq

21PH CALIBRATION FOR HI9218 & HI9219Procedure• Turn the instrument ON after connecting the pHelectrode and the temperature probe.• Immerse the tem

22••••• After about 30 seconds, the small display willshow "YES": press the CFM key to confirm thecalibration.The LCD will show "Err5&q

23PH CALIBRATION FOR HI9318Procedure••••• Switch the instrument on after connecting theelectrode and temperature probe.••••• Immerse the pH electrode

24The LCD will show "Err5" to indicate that the electrode is nowready for slope calibration.• Immerse the pH electrode and the probe intopH4

2520TEMP.ºCSAMPLEDATE°CDOWNºCUP20TEMPºC°C°C°CCALIBRATION WITH MANUAL TEMPERATURE COMPEN-SATIONIf for some reason the temperature probe is defective, o

26TEMPERATURE CALIBRATIONTEMPERATURE CALIBRATIONTEMPERATURE CALIBRATIONTEMPERATURE CALIBRATIONTEMPERATURE CALIBRATIONAll Hanna bench-top meters have b

27HOW TO SET DATE AND TIMEHOW TO SET DATE AND TIMEHOW TO SET DATE AND TIMEHOW TO SET DATE AND TIMEHOW TO SET DATE AND TIME(H(H(H(H(HIIIII9218 & H9

28OFFONin srum nsCONRANGE+/-CALTEMPENTERAENTERBCLEAR7894561230.PGMPROGRAMS OF HI9017PROGRAMS OF HI9017PROGRAMS OF HI9017PROGRAMS OF HI9017PROGRAMS OF

291PGMpHRANGE4 cm(1½")HI 7006The 6 programs stored in the instrument are:Program 1: To manually enter calibration buffer valuesProgram 2: To set

3HI9017, HI9218, HI9219 and HI9318 are microprocessor-based bench-top meters designed to meet the most stringent demands of the laboratory.They featur

30e.g. 6.95 at 5°C:• press 6• press decimal point• press 9• press 5• press ENTER AValue 6.95 appears on the left display with pH symbol blinking. Ifth

31PGM0pHCLEARThe left display value is transferred to the right display and the leftdisplay shows the temperature value.The instrument is now complete

32At this stage, the left display shows "P2-1", and the right displayshows the measured pH value.• press 9• press decimal point• press 3• pr

33RANGE3PGMmVE.g. activation of alarm for values higher than 500 mV and lower than-20.3 mV.• set the instrument to the mV mode• press 3• press PGM.At

34To stop:• press 0• press PGM.E.g. activation of alarm for values higher than 49.3°C and lower than-6.3°C.• press 4• press PGM.At this stage, the lef

35pHCLEARPGM0RANGE5PGMpHPROGRAM # 5 (HI 9017)Setting of endpoint and alert pH alarm values.When the alert value is reached i.e. between the final valu

36The left display then shows "P5-2".• press 9• press decimal point• press 0• press 3• press ENTER B.PROGRAM #6 (HI9017)Setting of RS232C ES

37PROGRAM 1A set sample no.B set timeC set dateSample number200The following section explains how each of the HI 9318's loggingprograms work.Each

383) The time value (B) can be set for a 24 hour clock. 2 P.M., forexample equals 14.00. Push "14.00" followed by "B".4) When sett

394 cm(1½")HI 7009PROGRAM #2 (HI9318)This program lets you calibrate with buffer values other than 4, 7 and10 pH which are pre-programmed into me

4(with 1m/3.3' cable), 12VDC adapter (HI710005 or HI710006),pH 4.01 & pH 7.01 buffer solutions (20 mL each), HI7071electrolyte solution (30

40B9 . 33PROGRAM 2A enter 1st buf- ferB enter 2nd buf- fer1st buffer6.922nd buffer9.33Check the appropriate value for the buffer at the measured buf

415PGMPROGRAM # 4 (HI9318)This program logs and prints pH/mV and temperature values at apreset interval between 1 minute and 24 hours.To enter the p

42The printout defines functions A, B and C:A is a start time,B is the time interval,C is the interrupt value ofpH/mV.Hours and minutes must besep

437PGMPROGRAM 7A select the lan-guage:1. English2. Deutch3. Français4. Español5. Italiano6. SvenskaFrançaisA3E.g. lower limit 6.5, upper limit 7.5.To

44PROGRAM #8 (HI9318)This program prints out the ion con-centration in M for the pH valuemeasured.To activate the program, press the 8key and then the

45TROUBLESHOOTING GUIDETROUBLESHOOTING GUIDETROUBLESHOOTING GUIDETROUBLESHOOTING GUIDETROUBLESHOOTING GUIDESymptoms are:The instrument doesnot work wi

46Data transmission from the instrument tothe PC is now much easier with the newHI92000 Windows® compatible applica-tion software offered by Hanna Ins

47This line makes the computer send a Data Link Escape character (thecommand expressed as a number or a 3-character sequence) and a CRcharacter.Note:

48BKY is equivalent to the B keyCKY is equivalent to pressing the C keyPGM is equivalent to pressing the PGM keyTEM is equivalent to pressing the TEMP

49HI9318 by pressing the 9 key and then the PGM key.Enter the ASCII Code of the desired prefix character and then press theENTER A key for HI9017 or t

5FRONT PANEL ANDFRONT PANEL ANDFRONT PANEL ANDFRONT PANEL ANDFRONT PANEL ANDSPECIFICATIONS OF HSPECIFICATIONS OF HSPECIFICATIONS OF HSPECIFICATIONS OF

50PREPARATIONRemove the protective cap.DO NOT BE ALARMED IF ANY SALT DEPOSITS ARE PRESENT.This is normal with electrodes and they will disappear when

51For refillable electrodes:If the filling solution (electrolyte) is more than 1 cm (½") below thefill hole, add HI7082 or HI8082 3,5M KCl Elect

52CLEANING PROCEDUREGeneral Soak in Hanna HI7061 or HI8061 General CleaningSolution for approximately 1 hour.Removal of films, dirt or deposits on the

53Alkaline Error1.0 Mol L-1 Na+0.1 Mol L-1 Na+Sodium Ion Correction for the Glass at 20-25°CConcentration pH Error13.0013.5014.0012.5013.0013.5014.0

54ACCESSORIESACCESSORIESACCESSORIESACCESSORIESACCESSORIESpH CALIBRATION SOLUTIONSHI 70004P pH 4.01 Buffer Sachets, 20mL, 25 pcsHI 70007P pH 7.01 Buffe

55REFILL ELECTROLYTE SOLUTIONS IN FDA APPROVED BOTTLESHI 8071 3.5M KCl + AgCl Electrolyte, 4x50mL, for single junc-tion electrodesHI 8072 1M KNO3 Elec

5675 mm2.95"6 mm0.25""S"VERSIONHI 2031120 mm4.7"12 mm0.5"9.5mm DIA0.37""S" VERSIONHI 1131120 mm4.7"5

57120 mm4.7"12 mm0.5""S" VERSIONHI 1332120 mm4.7"12 mm0.5"FC 10075 mm2.95"6 mm0.25"FC 200HI 1332B / HI1312SPla

58FC 911BPlastic-body (Kynar®), double junction, refillable with built-in ampli-fier, combination pH electrode. Use: very high humidity.HI 1413B / HI1

59HI5412Glass-body, single Calomel reference half-cell electrode, refillablewith 4mm plug with 1m (3.3') cable. Use: general purpose withconstan

6SPECIFICATIONS HI 9017Range pH 0.00 to 14.00ISE ± 399.9 mVORP ±1999 mV°C -10.0 to 125.0Resolution pH 0.01ISE 0.1 mVORP 1 mV°C 0.1Accuracy pH ±0.01(@

60Windows® is registered Trademark of "Microsoft Co."CONNECT TOSCREW TYPEELECTRODESCONNECT TO THEBNC SOCKETOF THE METERHI 7855 SERIES CABLE

61Application Electrodes1. Aquarium HI 1332B, HI 1911B, HI1312S2. Bath-water HI 1910B, HI 1130B, HI1110S3. Beer HI 1131B, HI 1111S4. Bread HI 2031B, F

62WARRANTYWARRANTYWARRANTYWARRANTYWARRANTYAll Hanna Instruments meters are warranted for two years againstdefects in workmanship and materials when us

63CE DECLARATION OF CONFORMITYCE DECLARATION OF CONFORMITYCE DECLARATION OF CONFORMITYCE DECLARATION OF CONFORMITYCE DECLARATION OF CONFORMITYDECLARAT

MANPHBN2R307/98http://www.hannainst.comPRINTED IN ITALYHANNA LITERATUREHANNA LITERATUREHANNA LITERATUREHANNA LITERATUREHANNA LITERATURELAB RECORDING W

7FRONT PANEL ANDFRONT PANEL ANDFRONT PANEL ANDFRONT PANEL ANDFRONT PANEL ANDSPECIFICATIONS OF HI9218 & HI9219SPECIFICATIONS OF HI9218 & HI9219

8SPECIFICATIONS HI9218 HI9219Ranges pH 0.00 to 14.00°C -10.0 to 125.0Resolution pH 0.01°C 0.1Accuracy pH ±0.01(@20°C/68°F) °C ±0.5Typical

9PAPERPRINT CLEARONOFFDATE RANGECALABC789456423+/- .PGMCON+/-TEMP.pH°Cin serum nsSAMPLE DATE0 PGM to exit from any program1 PGM to set sampling nu