Hanna-instruments HI 83212 Manual de usuario Pagina 22

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Silica
Place the cuvette into the holder and close the lid.
Press ZERO key. The display will show “-0.0-” when the
meter is zeroed and ready for measurement.
Remove the cuvette and add the content of one packet
of HI 93705C-0 Amino acid reagent and shake until it is
completely dissolved.
Reinsert the cuvette into the instrument.
Press TIMER and the display will show the countdown
prior to the measurement. Alternatively, wait for exactly 3
minutes and press READ. When the timer ends the meter
will perform the reading. The instrument displays
concentration in mg/L of silica (SiO
2
).
Press the s or t to access the second level of functions.
Press the Chem Frm functional key to convert the result in mg/L of Silicon (Si).
Press the s or t to go back to the measurement screen.
Silica
SILICA
SPECIFICATIONS
Range 0.00 to 2.00 mg/L
Resolution 0.01 mg/L
Accuracy ±0.03 mg/L ±3% of reading
Typical EMC ±0.01 mg/L
Deviation
Light Source Tungsten lamp with narrow band interference filter @ 610 nm
Method Adaptation of the
ASTM Manual of Water and Environmental Technology,
D859,
Heteropoly Blue method. The reaction between silica and reagents causes a blue tint in
the sample.
REQUIRED REAGENTS
Code Description Quantity
HI 93705A-0 Molybdate 6 drops
HI 93705B-0 Citric acid 1 packet
HI 93705C-0 Amino acid 1 packet
REAGENT SETS
HI 93705-01 Reagents for 100 tests
HI 93705-03 Reagents for 300 tests
For other accessories see page 50.
MEASUREMENT PROCEDURE
Select the
Silica
method using the procedure described in the
Method Selection
section (see page 12).
Fill the cuvette with 10 mL of unreacted sample (up to the
mark).
Add 6 drops of HI 93705A-0 Molybdate reagent. Replace the
cap and swirl the solution.
Wait for 4 minutes, add the content of one packet of HI 93705B-0
Citric acid reagent and shake until it is completely dissolved.
Wait for 1 minute. This is the blank.
10 mL
x 6
12
3
6
9
1’
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